How To Make Biodiesel
How To Make Biodiesel -
Introduction
Biodiesel
is generally made using chemicals to alter an organic oil by
using a catalyst and an alcohol (most people use ethanol or
methanol). Ethanol is less dangerous although methanol is not as
expensive. For the catalyst, sodium hydroxide (caustic soda) or
potassium hydroxide can be used, although sodium hydroxide is often
cheaper. The process of converting oil to biodiesel is called
Transesterification. The chemical reaction that occurs during this
process "cracks" the oil into Esters and Glycerol. As the
process occurs the glycerine gravitates to the bottom of the container
leaving alkyl esters, the glycerol is then drained off and the
remaining top liquid is biodiesel. The biodiesel is often then washed
to remove any remaining impurities and can then used to fuel an
unmodified diesel engine.
It is worth noting that pure biodiesel can dissolve natural
rubber hoses and seals. Most new diesel engines have synthetic hoses
and seals, but older engines may need to fitted with new hoses and
seals. Diesel injector pumps don't generally have rubber parts in
direct contact with the fuel, so it is usually easy to replace hoses
and seals without any major hassles. If a diluted fuel mixture of 20%
biodiesel and 80% petroleum diesel (called "B20") is used it should
have no effect on the older natural rubber hoses.
It is often recommended to make biodiesel from fresh oil to
gain an understanding and appreciation of the processes before moving
onto making bigger batches from waste oils. Biodiesel typically takes a
couple of days to a week from start to finish to making a batch. Most
people making biodiesel make anywhere between 20 to 100 gallons at a
time in a batch process.
Here's a breakdown of typical timing intervals from start to finish:
- START
- Collect Oil - 1-2 hours
- Filter Oil - 1-2 hours (depends on
amount of oil)
- Titration Of Oil - 10-15 minutes
- Transferring Oil To Processor - 10-20
minutes
- Heating Oil - 1-4 hours (depends on
amount of oil, voltage & wattage of element)
- Making Methoxide - 5-20 minutes (depends
on amount of methanol and catalyst used)
- Mixing Methoxide Into Oil - 20-30
minutes
- Mixing Oil & Methoxide - 2-3
hours
- Settling Oil - 8-10 hours (usually
overnight)
- Draining Glycerine - 5-10 minutes
- Transferring Biodiesel To Wash Tank -
10-20 minutes
- First
Mist Wash - 2-3 hours
- Second Mist Wash - 2-3 hours
- First Bubble Wash - 6-8 hours (usually
overnight)
- Second Bubble Wash - 6-8 hours (usually
overnight)
- Transferring Biodiesel To Drying Containers
- 10-20 minutes (depends on amount)
- Drying Biodiesel - 2 hours to 1 week
(depends heavily on weather and amount made)
- Transferring To Storage Containers -
10-20 minutes (depends on amount)
- FINISH
Equipment
Biodiesel
can be made in anything from a small 2 litre drink bottle to an
elaborate processor complete with separate tanks for processing,
washing, methoxide mixing, settling, and filtering. Obtaining equipment
is relatively easy. Complete processing equipment can be custom made
using plans off of the web or by buying pre-made kits ready to
assemble. Most people get started by making small batches with minimal
equipment and then gradually move up to making large batches using
large processors built specifically for making biodiesel.
Many home brewers either buy a variety of premade processors
designed for processing biodiesel or custom make
their own processors
either from kits or from plans on the web. Professionally built
processors can cost as little as $500 to several thousands of dollars.
Kits can be purchased for making your own from several online retailers
for as little as $200 on up to elaborate systems complete with methanol
recovery condensers.
Instructions
on How to Make Biodiesel
This
idea needs to be said again... Start with the
process, not with the processor. The processor
like the 250 litre (66 gallons) home made unit on the left
comes later. Start with fresh
unused oil, not with
waste vegetable oil (WVO) that also comes later. Understand the
process, start
by making a small, 1-litre test batch of biodiesel using fresh new oil.
You can
use a spare blender, or, better, make a simple Test-batch
mini-processor. Keep going, step by step. Study
everything you can. One of the best resources on the Web for detailed
instructions (it is free) is a site called Journey
to Forever.
Definitive Guide
- The Encylopedia of
Making Biodiesel
The
Encylopedia of Making Biodiesel is without doubt
the best book on the market (and we have looked at plenty) on how to
make biodiesel. David and Tram are the Managing Directors of
International Biofuel Solutions, and David is a lecturer at technical
universities in both Vietnam and Thailand. Over 200 pages of
step-by-step instructions with dozens of illustrations, drawings and
photographs to assist you. Whether you are just starting out or a
biodiesel pro, this book is really a must!
Biodiesel Recipes
Some links to detailed methods when thinking about
how to make biodiesel.
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